期刊
GREEN CHEMISTRY
卷 16, 期 3, 页码 1628-1632出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3gc41496e
关键词
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资金
- National Science Foundation [CHE-1058627]
- University of Cincinnati Research Council (URC)
Using a mechanically driven Diels-Alder reaction we were able to characterize the chemical energetics of a SPEX 8000M mixer/mill. Our results demonstrate that the conditions produced by this type of mill are similar to those produced when performing the same reaction at 90 degrees C in solution. Discrete element models and in situ temperature logging were used to analyse the energetics of this system. These models indicate that the yields obtained using a SPEX 8000M mill are best correlated to the velocity of the media and number of non-zero force collisions.
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