期刊
GREEN CHEMISTRY
卷 15, 期 9, 页码 2476-2484出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3gc40946e
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资金
- National Science Council, Taiwan [NSC 101-2113-M-005-008-MY3]
- National Chung Hsing University
- Center of Nanoscience and Nanotechnology (NCHU)
Copper-catalyzed C-S bond formation between aldehydes and thiols in the presence of TBHP as an oxidant is described. Functional groups including chloro, trifluoromethyl, bromo, iodo, nitrile, ester and thiophene are all tolerated by the reaction conditions employed. This reaction is performed in water without the use of a surfactant. Both aryl and alkyl aldehydes couple suitably with aryl- and alkyl thiols, affording the corresponding thioesters in moderate to good yields.
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