期刊
GREEN CHEMISTRY
卷 15, 期 4, 页码 1055-1060出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3gc00030c
关键词
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资金
- National Natural Science Foundation of China [21172200, 21102134]
- Innovation Fund for Outstanding Scholar of Henan Province [621001100]
An efficient and generally applicable protocol for the palladacycle-catalyzed arylation of diisopropyl H-phosphonate in water was developed. The remarkable features of this C-P bond-forming reaction include wide substrate scope including the inactive electron-rich and electron-neutral aryl chlorides, the weak inorganic base KF instead of strong bases such as (KOBu)-Bu-t or (NaOBu)-Bu-t for the activation of C-Cl bond, and the addition of isopropanol to avoid the decomposition of diisopropyl H-phosphonate.
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