期刊
GREEN CHEMISTRY
卷 13, 期 9, 页码 2543-2548出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1gc15400a
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Monomers used for the synthesis of terephthalate polyesters have been prepared starting from renewable resources. In particular, dimethyl terephthalate was synthesised starting from bio-limonene while butanediol was synthesised starting from bio-succinic acid. Using these bio-monomers it was possible to synthesise polyesters with the same chemical structure and molecular weight of commercially available polymers. Moreover, the polymers obtained from bio-based monomers, present the same thermal properties of the polyesters obtained using petrol-derived monomers. A poly(butylene terephthalate) completely obtained from renewable resources was also synthesised. The radiocarbon and isotope mass spectroscopy analysis confirmed that this polyester contains 94 +/- 3% of bio-based material.
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