期刊
GREEN CHEMISTRY
卷 12, 期 2, 页码 205-208出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/b921334a
关键词
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资金
- Major State Basic Resource Development Program [2003CB615807]
- NSFC [20973042, 20573024]
- Science and Technology Commission of Shanghai Municipality [08DZ2270500]
A new economic and green route to synthesize phthalide from 1,2-benzenedimethanol using aqueous hydrogen peroxide as the oxidant and tungstic acid as the catalyst under organic solvent-free conditions is presented. This process proceeds with advantages from the viewpoint of green chemistry, in which the only by-product of H2O2 is water and the catalyst can also be easily recovered. The desired product with high purity and good yield can be conveniently obtained when cooled after reaction.
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