期刊
FOOD CHEMISTRY
卷 122, 期 1, 页码 327-332出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2010.02.038
关键词
Gas chromatography-triple quadrupole mass spectrometry (GC-QqQ-MS/MS); Organophosphorous pesticide residues; Leeks; Dispersive solid phase extraction
A rapid multi-residue method was developed for the determination of 20 organophosphorous pesticide residues in leeks by gas chromatography coupled to triple quadrupole mass spectrometry (GC-QqQ-MS/MS). The method was based on the modified QuEChERS sample preparation method. After microwave pre-treatment, leek samples were extracted with acetonitrile containing acetic acid 0.1% and cleaned by dispersive solid phase extraction. The QqQ analyser acquired data in selected reaction monitoring (SRM) mode. Recoveries of 20 organophosphorous pesticides ranged from 81.0% to 109.4% with the relative standard deviations (RSD) below 10.4%. The limits of detection (LODs) were 0.07-1.5 mu g/kg. The limits of quantitation (LOQs) ranged from 0.25 to 5 mu g/kg. Ten leek samples were analysed for method application. (C) 2010 Elsevier Ltd. All rights reserved.
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