期刊
出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/02652030802342497
关键词
sterigmatocystin; mycotoxin; cheese; liquid chromatography-electrospray; positive; ionization-tandem; mass; spectrometry; (LC-MS; MS); Aspergillus spp; Aspergillus versicolor
资金
- ESF [VPD1/ESF/PIAA/04/NP/3.2.3.1./0001/0005/0067]
- European Commission
- ERASMUS [29-07/08]
Different cheese samples produced in Latvia (eight) and Belgium (13) were analysed for their sterigmatocystin (STC) content. Only two (9.5%) of the samples were positive for STC with concentration levels of 1.23 and 0.52 g kg-1, respectively. Five (24%) samples contained STC above the limit of detection (0.03 g kg-1) but below the limit of quantification (0.1 g kg-1), A sensitive liquid chromatography-electrospray positive ionisation-tandem mass spectrometry (LC-MS/MS) method, which was previously developed for the analysis of STC in grains, was modified and applied to the analysis of STC in cheese. This method involved sample extraction with acetonitrile-water (90 : 10, v/v), defatting with n-hexane, solid-phase extraction, separation on a reversed-phase C18 column, and STC detection by LC-MS/MS.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据