期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2014, 期 10, 页码 2032-2036出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201301833
关键词
Synthetic methods; Radical reactions; Alkenes; Oxygen; beta-Keto sulfones
资金
- Council of Scientific and Industrial Research (CSIR) [09/001(0379)/2013-EMR-I]
- Department of Science and Technology (DST) [SR/S1/OC-22/2010]
beta-Keto sulfones were obtained in good to excellent yields (73-94%) directly from unactivated olefins by employing inexpensive sodium arenesulfinate salts as sulfonylating agents and K2S2O8 as a radical initiator in open flasks and aqueous media at room temperature under transition-metal-free conditions. The reported oxidative sulfonylation protocol is highly practical and environmentally benign, as self-manifested by the extremely mild reaction conditions.
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