期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2013, 期 2, 页码 257-259出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201201126
关键词
Sulfur; Copper; Arenes; Cross-coupling
资金
- Institute for Advanced Studies in Basic Sciences (IASBS) Research Council [G2012IASBS156]
In this study, a protocol for the synthesis of symmetrical diaryl trithiocarbonates through the one-pot copper-catalyzed coupling reaction of sodium sulfide, carbon disulfide, and aryl compounds in DMF solution is presented. This method allows the synthesis of symmetrical diaryl trithiocarbonates without the use of highly toxic thiophosgene, and also, commercially available aryl halides were used instead of less available, toxic thiols.
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