期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2009, 期 36, 页码 6336-6340出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200900982
关键词
Arylation; Sulfides; Copper; Amino acids; Reaction mechanisms
资金
- Ministry of Education, Youth and Sports of the Czech Republic [LC06070, MSM 604 613 73 01, 2B08051]
A simple convenient method has been developed for the preparation of N-acetyl-S-arylcysteines based on the Chan-Lam-Evans arylation of N,N'-diacetylcystine dimethyl ester with arylboronic acids and used to synthesize a series of aryl-mercapturic acids. Unlike copper-mediated N-arylation, the S-arylation of neither cysteine nor cystine derivatives proceeded satisfactorily in the presence of air. ((C) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2009)
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