期刊
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
卷 21, 期 2, 页码 1326-1338出版社
SPRINGER HEIDELBERG
DOI: 10.1007/s11356-013-2022-1
关键词
GC-MS; Extraction; PAHs; Tea; QuEChERS; SPE sorbents
The aim of this work was the evaluation of QuEChERS extraction method for polycyclic aromatic hydrocarbon (PAH) determination in various types of tea. In the experiment, different kinds of extraction solvents, sorbents and a final method of sample preparation were compared. The final extracts were analysed by gas chromatography-selected ion monitoring-mass spectrometry. The results suggest that acetonitrile extraction, clean up with SAX and final liquid-liquid extraction was the best combination giving the most purified extracts and acceptable compound recoveries for different types of teas. In the study of real samples, compounds belonging to light PAHs were mostly detected, and heavy polycyclic aromatic hydrocarbons, including benzo[a]pyrene, were not identified in any of samples.
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