期刊
ELECTROPHORESIS
卷 32, 期 1, 页码 105-115出版社
WILEY
DOI: 10.1002/elps.201000349
关键词
CEC; Enzymatic reactor; Hybrid monolith; Micro-HPLC; SPME
资金
- National Natural Science Foundation of China [20735004, 20875089]
- State Key Basic Research Development Program of China [2005CB522701]
- National High Technology Research and Development Program of China [2008AA02Z211]
- Chinese Academy of Sciences [KSCXZ-YW-G-046]
Organic-silica hybrid monolithic columns have drawn more and more attention due to the ease of preparation and good mechanical stability in recent years. Many synthetic approaches have been developed and a variety of hybrid monolithic capillary columns have been prepared. The sol-gel process is well recognized in the fabrication of hybrid monolithic columns, which can be mainly classified as one-step, acid/base two-step procedures. The new approaches such as the one-pot'' and nano-scaled inorganic-organic hybrid reagent of polyhedral oligomeric silsesquioxane used as a cross-linker have also emerged for the preparation of hybrid monolithic columns. The applications of the organic-silica hybrid monolithic capillary columns for capillary electrochromatography, micro high-performance liquid chromatography, solid-phase microextraction and enzymatic reactor etc. are included in this review.
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