期刊
ELECTROCHIMICA ACTA
卷 53, 期 15, 页码 4990-4997出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.electacta.2008.02.020
关键词
polypyrrole; carbon nanotubes; ionic liquids; electrochemical capacitance; composites
Composites of polypyrrole (PPy) and multi-walled carbon nanotubes (MWCNTs) were synthesized by a facile method involving one-step electrochemical deposition from a thin-layer of ionic liquid solution attached on a glassy carbon electrode. The morphology of the composites was characterized by field emission scanning electron microscopy, and the capacitance properties were investigated by cyclic voltammetry (CV). The charge-discharge behavior of the composites prepared in this work was examined by chronopotentiometry at a constant current density for multi-cycle scans. The results show that the PPy/MWCNT composites have a porous 3D nanostructure, with high specific capacitance (SC) of 890 F/g (for the mass of the PPy in the composites) calculated from CV at 2 mV/s in 1.0 M KCl. The stability of the composites in 1.0 M KCl electrolyte was also examined by multi-cycle CV and only 9% decrease of SC value was observed for the 1000 cycles. (C) 2008 Elsevier Ltd. All rights reserved.
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