期刊
ELECTROCHIMICA ACTA
卷 53, 期 7, 页码 3139-3148出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.electacta.2007.11.046
关键词
manganese phthalocyanine; titanium phthalocyanine; cyclic voltammetry; spectroelectrochemistry; electrocatalysis; nitrite
This work reports on the synthesis of manganese and titanium phthatocyanine complexes that are tetra-substituted at four non-peripheral positions with amino ligands. The complexes are investigated for the first time for their electrochemical properties using cyclic voltammetry, rotating disc electrode voltammetry and spectroelectrochemistry. Electropolymerisation on a glassy carbon electrode was performed with ease and the modified electrodes were investigated for electrocatalysis of nitrite oxidation. Nitrite oxidation to nitrate is confirmed from the transfer of a total of two electrons. (C) 2007 Elsevier Ltd. All rights reserved.
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