期刊
ELECTROANALYSIS
卷 26, 期 5, 页码 1059-1067出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/elan.201300653
关键词
Gels; Conducting materials; Ion pairs; Electrochemical impedance spectroscopy; Protective coatings
资金
- National Science Foundation [1139230]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1139230] Funding Source: National Science Foundation
A novel conductive anionic hydrogel was synthesized for use as a solid electrolyte for electrochemical impedance spectroscopy (EIS) characterization of the barrier properties of protective coatings on outdoor metalworks, such as bronze sculptures. The AMPS-co-PAA hydrogel was soaked in a variety of aqueous salt solutions and characterized by swelling capacity and conductivity in order to determine the most appropriate gel/liquid electrolyte combination for use on culturally significant objects. K2PIPES-equilibrated hydrogels were selected as the preferred electrodes for this particular application and were used to measure the impedance of a coated substrate, yielding spectra similar to those from standard liquid cells.
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