期刊
DYES AND PIGMENTS
卷 79, 期 3, 页码 247-251出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.dyepig.2008.03.004
关键词
phthalocyanines; phthalonitrile derivatives; magnesium; soluble; tert-butyl groups; synthesis
A phthalonitrile derivative bearing 2,4-di-tert-butylphenoxy substituents at peripheral positions was synthesized; subsequent cyclotetramerization in DMF and hexanol furnished the desired zinc (II), magnesium (II), copper (II) and nickel (II) phthalocyanines. These metallo-phthalocyanines were highly soluble in solvents such as dichloromethane, chloroform, acetone, ethyl acetate, tetrahydrofuran, diethyl ether, n-hexane and DMF. The structures of the compounds were confirmed by elemental analyses, IR, H-1 NMR, C-13 NMR, electronic spectra and mass spectroscopic methods. (C) 2008 Elsevier Ltd. All rights reserved.
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