期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 80, 期 14, 页码 7266-7274出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b00853
关键词
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Here, we report accessing small 3-fluoropyrrolidines and 3,3-difluoropyrrolidines through a 1,3-dipolar cycloaddition with a simple azomethine ylide and a variety of vinyl fluorides and vinyl difluorides. We demonstrate that vinyl fluorides within alpha,beta-unsaturated, styrenyl and even enol ether systems can participate in the cycloaddition reaction. The vinyl fluorides are relatively easy to synthesize through a variety of methods, making the 3-fluoropyrrolidines very accessible.
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