期刊
DESALINATION AND WATER TREATMENT
卷 52, 期 4-6, 页码 1177-1182出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/19443994.2013.827310
关键词
Soil; Prometryne; Acetochlor; Solid-phase extraction; Gas chromatography-mass spectrometer
资金
- Program for Innovative Research Team (in Science and Technology) in University of Yunnan Province (IRTSTYN), Green Chemistry and Functional Materials Research for Yunnan Innovation Team [2011HC008]
A highly sensitive and simple analytical method was developed for analyzing the binary mixed pesticides of prometryne and acetochlor in soil-water system by gas chromatography/mass spectrometry (GC/MS). The sample solution was first purified by C-18 solid-phase extraction column, which was leached by acetone. The leachate was enriched to 1.0mL by pressure blowing concentrator and then analyzed by GC/MS. The linear calibration curves were showed in the range of 1-15g/mL with a correlation coefficient of 0.9991. The average recoveries (n=5) were between 95.3 and 115.7%, with relative standard deviations ranged from 1.71 and 7.95%. The limits of detection of Prometryne/Acetochlor were up to 0.06 and 0.17g/mL, respectively. This method provides a reliable approach to examine and evaluate the residues of prometryne and acetochlor in the soil-water system.
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