4.5 Article

HR-MAS NMR Spectroscopy: A Practical Guide for Natural Samples

期刊

CURRENT ORGANIC CHEMISTRY
卷 17, 期 24, 页码 3013-3031

出版社

BENTHAM SCIENCE PUBL LTD
DOI: 10.2174/13852728113179990126

关键词

1D NMR; 2D NMR; Algae; High resolution magic angle spinning (HR-MAS); Natural samples; NMR; Soils; Worm tissue

资金

  1. NSERC
  2. Canada Foundation for Innovation (CFI)
  3. Ministry of Research and Innovation (MRI)
  4. Government of Ontario

向作者/读者索取更多资源

High Resolution Magic Angle Spinning (HR-MAS) NMR spectroscopy is a versatile technique that provides high resolution NMR data on samples containing solutions, gels and swellable solids. In addition to providing structural information HR-MAS can also be used to investigate interfaces (for example organic structures at the solid-aqueous soil interface), processes such as swelling/flocculation, kinetic transfer between gel/liquid phases, as well as conformation and molecular interactions in situ. As such, HRMAS has potential in a diversity of fields including organic, biological, environmental, and medical research. This manuscript focuses on the application of HR-MAS to intact natural samples. A range of 1D and 2D NMR experiments are reviewed and compared in terms of general performance on a range of samples. Therefore, this practical guide and review should be a useful reference and starting point for those wishing to apply HR-MAS NMR. While this article focuses on natural samples, common key 1D and 2D experiments are considered which may be of interest to readers with diverse research interests.

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