期刊
COMPOSITES SCIENCE AND TECHNOLOGY
卷 70, 期 12, 页码 1704-1712出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.compscitech.2010.06.016
关键词
Wood; Mechanical properties; CP/MAS C-13 NMR; Heat treatment; Isostatic pressing
All-cellulose composites are commonly prepared using cellulose solvents. In this study, moldable all-cellulose I wood fiber materials of high cellulose purity (97%) were successfully compression molded. Water is the only processing aid. The material is interesting as a green biocomposite for industrial applications. Dissolving wood fiber pulps (Eucalyptus hardwood and conifer softwood) are used and the influence of pulp origin, beating and pressing temperature (20-180 degrees C) on supramolecular cellulose nanostructure is studied by solid state CP/MAS C-13 NMR. Average molar mass is determined by SEC to assess process degradation effects. Mechanical properties are determined in tensile tests. High-density composites were obtained with a Young's modulus of up to 13 GPa. In addition, nanoscale cellulose fibril aggregation was confirmed due to processing, and resulted in a less moisture sensitive material. (c) 2010 Elsevier Ltd. All rights reserved.
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