期刊
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
卷 54, 期 9, 页码 2766-2770出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201409663
关键词
cycloaddition; continuous micro flow-through; electrophoresis; mass spectrometry; microfluidics
资金
- LIFE-Leipzig Research Center for Civilization Diseases, Universitat Leipzig
- European Social Fund
- Free State of Saxony
Free-flow electrophoresis is an ideal tool for preparative separations in continuous microflow. With the approach presented herein for coupling free-flow electrophoresis and mass spectrometry it is now also possible to trace non-fluorescent compounds and identify them by means of mass spectrometry. The functionality of the method and its potential as an integrated separation unit for microflow synthesis is demonstrated by application to a multicomponent [3+2]-cycloannulation.
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