期刊
CHROMATOGRAPHIA
卷 67, 期 5-6, 页码 425-431出版社
SPRINGER HEIDELBERG
DOI: 10.1365/s10337-007-0514-1
关键词
GC-MS; solid-phase microextraction; preservatives and antioxidants; cosmetics
A rapid and simple procedure for the determination of antioxidants and preservatives in cosmetics has been developed utilizing solid-phase microextraction combined with GC-MS. A silica fiber coated with polyacrylate provided the highest extraction efficiency. Detection limits in the range from 0.4 to 8.5 ng mL(-1) were obtained. Linearity is over a wide range from 1 to 2,000 ng mL(-1) with a relative standard deviation under 16%. Cosmetic from a local supermarket were analysed for antioxidants and preservatives to demonstrate the effectiveness of the proposed method. The concentration of antioxidants and preservatives determined was 20-1,218 mu g g(-1) for methylparaben and 5-3,779 mu g g(-1) for propylparaben.
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