期刊
CHINESE SCIENCE BULLETIN
卷 58, 期 10, 页码 1156-1161出版社
SCIENCE PRESS
DOI: 10.1007/s11434-012-5637-6
关键词
TiO2 nanotube; microcystin; photocatalysis; sunlight irradiation
资金
- National Natural Science Foundation of China [20906097]
- Natural Science Foundation of Jiangsu Province, China [BK2011881]
In order to investigate the catalytic performance of anodic TiO2 nanotubes and their practical application in the treatment of refractory microcystins (MCs) in natural-water samples, TiO2 nanotubes of diameter of 50-80 nm were fabricated by anodization in C2H2O4 center dot 2H(2)O containing NH4F. Under irradiation with natural sunlight, MC-LR was totally degraded after 1 d using the anodic TiO2 nanotubes. In contrast, the removal efficiency without TiO2 nanotubes was as low as 47.7% within 20 d. In addition, a mixture of anatase and rutile TiO2 gave higher photocatalytic activity than the single phase did. The pH also influenced the adsorption capacity of the TiO2 nanotubes. The order of MC-LR degradation efficiencies at different pH values was 3.5 > 8.0 > 10.0. After five repeated experiments on the degradation of MC-LR for 7 h, the degradation efficiency was still stable.
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