期刊
CHINESE CHEMICAL LETTERS
卷 20, 期 2, 页码 127-130出版社
ELSEVIER SCIENCE INC
DOI: 10.1016/j.cclet.2008.11.002
关键词
Allyloxycarbonyl group; Orthogonal protective strategy; Carbohydretes
资金
- Foundation of Ministry of Education of China [20070019072]
- Research Foundation of China Agricultural University [90020031]
Highly efficient removal of allyloxycarbonyl (Alloc) group was achieved in the presence of CH3COONH4, Pd[P(C6H5)(3)](4), and NaBH4 in MeOH-THF, within 5 min in almost quantitative yields (>90%, isolated yield) without affecting acetyl, benzoyl, isopropylidene, benzylidene, allyl, benzyl, benzyl carbonate, or azido groups. (C) 2008 Jian Jun Zhang. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
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