期刊
CHEMISTRY-A EUROPEAN JOURNAL
卷 20, 期 52, 页码 17635-17639出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201405057
关键词
anilines; ketones; metal-free reactions; synthetic methods; 1,2,3-triazoles
资金
- Natural Science Foundation of China [21272205]
- National Basic Research Program of China [2011CB936003]
- Program for the Zhejiang Leading Team of Science and Technology Innovation [2011R50007]
A novel synthetic approach toward 1,4-disubstituted 1,2,3-triazoles by C-N- and N-N-bond formation has been established under transition-metal-free conditions. Complete control of the regioselectivity was successfully achieved. Commercially available anilines, ketones, and N-tosylhydrazine were treated with molecular iodine in one pot to allow the regioselective generation of 1,4-disubstituted 1,2,3-triazoles in high yields without the use of azides.
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