期刊
CHEMISTRY LETTERS
卷 41, 期 6, 页码 628-629出版社
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2012.628
关键词
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资金
- Grants-in-Aid for Scientific Research [21106001, 23350017, 21106005] Funding Source: KAKEN
Treatment of 1,6-dialkylhexa-1,5-diene-3,4-diones with bis(iodozincio)methane at -78 degrees C for several hours gave cis-dialkenylcyclopropane-1,2-diols which rearranged into the zinc alkoxides of cis-5,6-dialkylcyclohepta-3,7-diene-1,3-diol in good yields at room temperature as a one-pot reaction. The reaction should be performed under the careful temperature control. When the reaction was performed using a microflow system, these two-step reactions were able to be performed in a few seconds at room temperature.
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