4.7 Article

Preparation of a novel ultra-high temperature low-damage fracturing fluid system using dynamic crosslinking strategy

期刊

CHEMICAL ENGINEERING JOURNAL
卷 354, 期 -, 页码 913-921

出版社

ELSEVIER SCIENCE SA
DOI: 10.1016/j.cej.2018.08.021

关键词

Hydrophobically associating water-soluble polymer; Fracturing fluid; Polyethylenimine; Ultra-high temperature; Dynamic crosslinking

资金

  1. Sichuan Youth Science & Technology Foundation [2017JQ0010]
  2. National High Technology Research & Development Program [2016ZX05053]
  3. Key Fund Project of Educational Commission of Sichuan Province [16CZ0008]
  4. Explorative Project Fund of State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation (Southwest Petroleum University) [G201601]
  5. Major Program of the National Natural Science Foundation of China [51490653]
  6. 973 Program [2013CB228004]

向作者/读者索取更多资源

Novel polymer-based fracturing fluid was developed to exploit ultra-high temperature reservoirs. SEM and rheology studies suggest that this gel system with rigid spatial network structure could be healed by the interaction between polyethylenimine and polymer at high temperature. According to the reaction kinetics, the function of gelling time with temperature was obtained. The viscoelasticity and thixotropy behaviors have been investigated. The maximum temperature that fluid could bear was up to 220 degrees C (170 s(-1)), and up to 260 degrees C (100 s(-1)) after being sheared for 120 min. The shear recovery test indicated that the fluid displayed excellent shear recovery properties at 180 degrees C. The settling rate of proppants and filtration rate of the fluid were 1.401 min/cm and 0.2637 x 10(-5) m/min at 180 degrees C, respectively. The viscosity of the transparent breaking liquid was 2.4 mPa center dot s. Thus, this practical fracturing fluid could be an alternative for the development of oil & gas resources in deep wells.

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