期刊
CHEMICAL COMMUNICATIONS
卷 54, 期 66, 页码 9147-9150出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8cc04428g
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The rhodium(iii)-catalyzed intramolecular annulation of alkyne-tethered 3-(indol-3-yl)-3-oxopropanenitriles for the synthesis of fused carbazole scaffolds via C-H activation has been developed. A series of six-, seven-, and eight-membered hydroazepino[3,2,1-jk]carbazoles were achieved. This reaction proceeded under mild reaction conditions and with a broad substrate scope. The reaction involved sequential cleavage of C(sp(2))-H/C(sp(3))-H bonds and annulation with the tethered alkyne.
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