期刊
CHEMICAL COMMUNICATIONS
卷 50, 期 60, 页码 8148-8150出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc03470h
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资金
- JSPS KAKENHI [22350017, 24550048, 24655028, 24109013]
- Grants for Excellent Graduate Schools, MEXT, Japan
- Molecular Systems Research project of RIKEN Advanced Science Institute
- Kyoto Technoscience Center
- Research Institute for Production Development
A stable 1-bromoalumole has been synthesized by the reaction of a 1,4-dilithio-1,3-butadiene derivative with AlBr3. The 1-bromoalumole was found to exist as a dimeric structure in the crystalline state. Reaction of the 1-bromoalumole with Mes*Li afforded the corresponding Mes*-substituted alumole (Mes* = 2,4,6-(t-Bu)(3)C6H2), demonstrating the potential of the 1-bromoalumole for the functionalization of alumoles.
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