期刊
CHEMICAL COMMUNICATIONS
卷 50, 期 73, 页码 10588-10591出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc04959d
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资金
- AstraZeneca
- Royal Society
- EPSRC [EP/J001872/1, EP/L001497/1, EP/K001183/1]
- University of Strathclyde
- Engineering and Physical Sciences Research Council [EP/L001497/1, EP/J001872/1, EP/K001183/1] Funding Source: researchfish
A general thermolysis reaction for the transformation of Group 1 TMP compounds (LiTMP, NaTMP, KTMP) to 1-aza-allylic TTHP derivatives is reported. TMEDA accelerates the reaction and produces the crystalline complexes [(TMEDA) LiTTHP] and [(TMEDA.NaTTHP)(2)]. Methane elimination during the transformational process was confirmed via TVA coupled to MS.
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