期刊
CHEMICAL COMMUNICATIONS
卷 50, 期 95, 页码 15059-15062出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc07058e
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资金
- Platform for Drug Discovery, Informatics, and Structural Life Science from MEXT, Japan
- JSPS KAKENHI [24310164, 26350971]
- Kurata Memorial Hitachi Science and Technology Foundation
- Sumitomo Electric Group Corporate Social Responsibility Foundation
- Cooperative Research Program of the Network Joint Research Center for Materials and Devices (IMCE, Kyushu University)
3-Triflyloxybenzynewas generated via an iodine-magnesium exchange reaction of 1,3-bis(triflyloxy)-2-iodobenzene using the trimethylsilylmethyl Grignard reagent. Various arynophiles and nucleophiles reacted regioselectively with 3-triflyoxybenzyne to afford cycloadducts and unique aryl triflones, which were provided via thia-Fries rearrangement.
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