期刊
CHEMICAL COMMUNICATIONS
卷 49, 期 66, 页码 7316-7318出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc43456g
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资金
- DST (Nanomission)
- DST, New Delhi, Govt of India [SR/S1/PC-07/2011(G)]
A facile precursor dependent single step, one pot solution based synthesis of wurtzite and chalcopyrite polymorphs of CuFeS2 has been developed by reacting a Cu(I) thiourea complex with Fe-2(SO4)(3) and FeCl3 separately in ethylene glycol. The phases have been characterized by structural refinements, SEM-EDX, TEM-SAED, Raman, UV-Visible spectroscopy and TGA measurements.
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