期刊
CHEMICAL COMMUNICATIONS
卷 48, 期 41, 页码 4977-4979出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc31601c
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资金
- University of Pennsylvania
- University Research Foundation
- United States National Science Foundation MRSEC [DMR-1120901]
- NSF [CHE-0840438, CHE-0131132]
- Division Of Materials Research
- Direct For Mathematical & Physical Scien [1120901] Funding Source: National Science Foundation
Pentavalent uranium complexes of the formula (UX2)-X-v[N(SiMe3)(2)](3) (X = F-, Cl-, Br-, N-3(-), NCS-) are accessible from the oxidation of U-III[N(SiMe3)(2)](3) through two sequential, one-electron oxidation reactions (halides) and substitution through salt metathesis (pseudohalides). Uranium(v) mixed-halides are also synthesized by successive one-electron oxidation reactions.
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