4.7 Article

TBHP-mediated oxidative thiolation of an sp(3) C-H bond adjacent to a nitrogen atom in an amide

期刊

CHEMICAL COMMUNICATIONS
卷 47, 期 48, 页码 12867-12869

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ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc15397h

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资金

  1. NSFC [21172060]
  2. DSTF of Hunan [2009WK4005]
  3. DSTF of Changsha [K0802152-31]

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The first example of molecular sieve-promoted TBHP-mediated direct oxidative thiolation of an sp(3) C-H bond adjacent to a nitrogen atom with disulfides under metal-free conditions, which allows for preparation of numerous S,N-containing compounds, is presented. Moreover, diverse benzothiazoles and a fipronil analog can be synthesized through this strategy.

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