期刊
CHEMICAL COMMUNICATIONS
卷 47, 期 29, 页码 8265-8267出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc13016a
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资金
- European Research Council [GO802567]
- EPSRC [BB/F007426/1]
- BBSRC [BB/F007426/1] Funding Source: UKRI
- Biotechnology and Biological Sciences Research Council [BB/F007426/1] Funding Source: researchfish
Preparation of the all-syn isomer of 1,2,3,4-tetrafluorocyclohexane is reported; X-ray structural studies shows a conformation with two of the C-F bonds oriented 1,3-diaxial to each other and (19)F-NMR reveals a through space diaxial (4)J(FF) coupling constant of 29 Hz.
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