期刊
CHEMICAL COMMUNICATIONS
卷 47, 期 23, 页码 6686-6688出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc11906k
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资金
- National Science Council, Republic of China
- Academia Sinica
Complexes [Cu(NPh(2))(2)](-), [Cu(NPh(2))I](-) and K[ Cu(phen)(NPh(2)) (p-tolyl)](+) were observed by in situ electrospray ionization mass spectrometry (ESI-MS) analysis of the copper(I)-catalyzed C-N coupling reaction under the catalytic reaction condition indicating that they are intermediates in the reaction. A catalytic cycle composed of a free radical path and a 2e oxidative addition path is proposed based on these observations.
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