期刊
CHEMICAL COMMUNICATIONS
卷 47, 期 20, 页码 5846-5848出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc11025j
关键词
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资金
- Merck
- EPSRC
Ionic liquids have been used in combination with ball milling on a range of chlorophosphoramidite reagents to phosphitylate nucleosides and 2-deoxynucleosides. The enhanced stability offered by the ionic liquid mediated processes combined with efficient mass transfer induced by ball milling has enabled excellent yields to be obtained even when using small dialkyl amino groups as well as the more commonly used diisopropylamino protection.
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