期刊
CHEMICAL COMMUNICATIONS
卷 46, 期 39, 页码 7424-7426出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0cc01732a
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We report a simple and rapid microwave-assisted method for the preparation of oligosaccharide-glycosylamines, followed by labelling with tris(2,4,6-trimethoxyphenyl) phosphonium acetic acid N-hydroxysuccinimide ester. The facile strategy introduced a permanent charge at the reducing end of the oligosaccharide. In combination of MALDI-MS, the detection limit for maltoheptaose was as low as 2 fmol mu L(-1).
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