期刊
CHEMICAL COMMUNICATIONS
卷 46, 期 34, 页码 6350-6352出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0cc01980a
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An operationally simple iron-catalyzed hydrodehalogenation of aryl halides has been developed with 1 mol% Fe(acac) 3 and commercial t-BuMgCl as reductant. The mild reaction conditions (THF, 0 degrees C, 1.5 h) effect rapid chemoselective dehalogenation of (hetero) aryl halides (I, Br, Cl) and tolerate F, Cl, OR, SR, CN, CO2R, and vinyl groups.
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