期刊
CHEMICAL COMMUNICATIONS
卷 46, 期 46, 页码 8722-8724出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0cc02239j
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- NEDO, Japan
A highly efficient, two-stage, continuous-flow synthesis of vitamin D-3 from provitamin D-3 was achieved. The developed method afforded the desired product in high yield (HPLC-UV: 60%, isolated: 32%) and required neither intermediate purification nor high-dilution conditions.
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