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Toward benign syntheses of pyridines involving sequential solvent free aldol and Michael addition reactions

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CHEMICAL COMMUNICATIONS
卷 -, 期 22, 页码 2199-2200

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ROYAL SOC CHEMISTRY
DOI: 10.1039/b007431o

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Krohnke type pyridines are readily accessible via a sequential solventless aldol condensation and Michael addition involving solid NaOH, followed by treatment with ammonium acetate in acetic acid, as a one pot reaction, which enables both symmetrical and unsymmetrical 2,6-bisaryl substituted pyridines to be isolated in high yield, typically > 75%.

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