期刊
POLYMER
卷 41, 期 2, 页码 565-574出版社
ELSEVIER SCI LTD
DOI: 10.1016/S0032-3861(99)00210-4
关键词
FT-NIR spectroscopy; epoxy resins; diffusion
An epoxy resin formulation composed of tetraglycidyl-4,4'-diamino diphenylmethane (TGDDM) and 4,4'diamino diphenyl sulfone (DDS) was investigated by Fourier transform near infrared (FT-NIR) spectroscopy and dynamic-mechanical analysis. Both techniques have demonstrated the essentially complete cure state of the resin with the adopted curing schedule. A novel feature of this work is the possibility of monitoring the transport of water into the resin by using of an FT-MIR spectrometer as a detector in place of the currently employed gravimetric detectors. The data gathered at different temperatures have revealed a good agreement with conventional gravimetric measurements, which verifies the reliability and accuracy of the experimental approach presented herein. (C) 1999 Elsevier Science Ltd. All rights reserved.
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