期刊
CHEMICAL & PHARMACEUTICAL BULLETIN
卷 60, 期 7, 页码 854-858出版社
PHARMACEUTICAL SOC JAPAN
DOI: 10.1248/cpb.c12-00160
关键词
one pot synthesis; antioxidant activity; antimicrobial activity
资金
- BRNS, Mumbai [2010/37C/26/BRNS/1424]
A simple and efficient one pot synthesis of 2-amino-4H-chromen-4-yl phosphonate derivatives has been accomplished by the condensation of salicylaldehyde, malononitrile/ethylcyanoacetate and triethyl phosphite/trimethyl phosphite in the presence of molecular iodine as catalyst in water at room temperature. All the reactions were very clean and the products were obtained in very good to excellent yields. The title compounds are characterized by IR, H-1, C-13-, P-31-NMR and mass spectra, also studied their antimicrobial and antioxidant activity.
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