期刊
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
卷 -, 期 3, 页码 395-400出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/a906832e
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Treatment of an alkyne with iodine monochloride and sodium iodide at room temperature results in the formation of the thermodynamic (E)-diiodoalkene. The corresponding (Z)-diiodoalkene can also be produced, by treatment of the alkyne with iodine monochloride at -78 degrees C in the presence of tetraethylammonium iodide. Such 1,2-diiodoalkenes are useful for the synthesis of more functionalised alkenes by using either Stille or Suzuki cross-coupling protocols.
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