期刊
JOURNAL OF SOLID STATE CHEMISTRY
卷 149, 期 1, 页码 88-91出版社
ACADEMIC PRESS INC
DOI: 10.1006/jssc.1999.8499
关键词
solvothermal process; metal phosphides; ethylene-diamine; nanocrystals
Nanocrystalline Co2P Ni2P, and Cu3P were successfully prepared through a simple solvothermal process based on the direct reactions of metal halides with yellow phosphorus at rather mild temperatures (80-140 degrees C) with ethylenediamine used as the solvent, XRD, XPS, and TEM were used to study the phases, compositions, and morphologies of the final products, A possible mechanism is proposed and the influential factors in the process are discussed in detail. (C) 2000 Academic Press.
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