期刊
SYNTHETIC COMMUNICATIONS
卷 30, 期 4, 页码 597-607出版社
MARCEL DEKKER INC
DOI: 10.1080/00397910008087361
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Samarium (II) iodide has been successfully utilized as a strong one-electron on transfer reducing agent for the cyclodimerization of alpha, beta-unsaturated ketones. The absence of any alcohol as proton source is essential. The reaction is regioselective over the competitive carbon-carbon double bond reduction and stereocontrolled. The configuration of the cyclodimerization products, has been confirmed by X-ray analysis.
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