期刊
SYNTHETIC COMMUNICATIONS
卷 32, 期 3, 页码 319-328出版社
MARCEL DEKKER INC
DOI: 10.1081/SCC-120002114
关键词
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A major problem in the use of spermidine for the synthesis of biologically interesting compounds is the selective orthogonal protection of the three different amino groups. Our approach is based on the Fukuyama reaction, starting from putrescine and 3-amino-1-propanol and affording N-8-benzyloxycarbonyl-N-1-tert-butyloxycarbonyl-N-4-(2-nitro-benzenesulfonyl)spermidine (5) in 5 steps in high yield.
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