期刊
JOURNAL OF THE AMERICAN CERAMIC SOCIETY
卷 86, 期 1, 页码 206-208出版社
AMER CERAMIC SOC
DOI: 10.1111/j.1151-2916.2003.tb03308.x
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Titanium nitride (TiN) particles (8 nm) were prepared via a reduction-nitridation route in an autoclave at 500degreesC, using TiCl4, NH4Cl, and metal Na as reactants. X-ray powder diffraction indicated that the product was a NaCl-type of TiN with a cell constant a = 4.242 Angstrom. Transmission electron microscopy images showed that the TiN particles were 5-10 mn. Raman spectra showed the defect-induced first-order shifts in the TiN nanocrystals.
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