期刊
RAPID COMMUNICATIONS IN MASS SPECTROMETRY
卷 18, 期 17, 页码 1965-1971出版社
WILEY
DOI: 10.1002/rcm.1577
关键词
-
A method based on liquid chromatography with electrospray ionisation ion trap mass spectrometry, for the determination of ochratoxin A (OTA) in meat products using ochratoxin B (OTB) as an internal standard, is described. Fragmentation patterns of OTA and OTB were studied by sequential mass spectrometry. Trace determination was then accomplished by consecutive reaction monitoring (CRM) of a fragment obtained by MS3 experiments. This led to a better signal-to-noise ratio and to a higher specificity of the technique. The response to OTA was linear over at least one concentration decade with a limit of detection of 0.6 ng/g. The method was applied to pig tissue samples naturally contaminated by OTA. Copyright (C) 2004 John Wiley Sons, Ltd.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据