期刊
MOLECULES
卷 10, 期 1, 页码 183-189出版社
MDPI
DOI: 10.3390/10010183
关键词
ring-enlargement; cyclic ether; hypervalent iodine compounds
Stereoselective synthesis of 5-7 membered cyclic ethers was achieved by deiodonative ring-enlargement of cyclic ethers having an iodoalkyl substituent. The reaction took place readily under mild conditions using hypervalent iodine compounds and an acetoxy or a trifluoroacetoxy group was introduced into the rings depending on the hypervalent iodine reagent employed. The use of hexafluoroisopropanol (HFIP) as solvent is critical.
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